Preparation and characterization of new compounds for esters and polymers derived from furfural, study of some physical applications and evaluation of their biological activity

Mohammed Rashed Wajih Al-Ani; Nabil Jamal Ayed, AlAsli

doi:10.53730/ijhs.v6nS1.8895

Authors

Mohammed Rashed Wajih Al-Ani Chemistry Department - College of Education for Pure Sciences - Tikrit University. Salah Al-Din – Iraq
Nabil Jamal Ayed, AlAsli Chemistry Department - College of Education for Pure Sciences - Tikrit University. Salah Al-Din – Iraq

Keywords:

Furfural, Schiff's bases, Amic acids, Esters, Pseudomonas Putida, Klebsiella Pneumoniae, Staphylococcus Aureus, Enterococcus

Abstract

This research includes the preparation of esters and loading of polymers through the reaction of amino acids derived from furfural with alcohols and polyvinyl alcohol by the traditional method (sublimation). 1:1 mol) and then reacts the product of Schiff's bases with the anhydride. The compounds were diagnosed using infrared spectroscopy (IR), nuclear magnetic resonance (¹H, ¹³C-NMR), UV-Vis spectroscopy, and mass spectrometry (Mass). Laser bombardment was also performed using a scanning electron microscope (SEM) to determine the shape of the particle and whether it was a nanoparticle or not. Also, the biological activity was evaluated on four types of karma-positive and gram-negative pathogenic bacteria, which showed moderate to high inhibitory ratios and measured the molar electrical conductivity of some of them. The products were confirmed by the physical changes that occurred to them, such as color, molecular weight, and melting point.

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